Crystallography Open Database

Information card for entry 2209263

2209262 << 2209263 >> 2209264

Preview

Structure parameters

Chemical name	trans-carbonylchlorobis[tris(4-fluorophenyl)phosphine]rhodium(I)
Formula	C37 H24 Cl F6 O P2 Rh
Calculated formula	C37 H24 Cl F6 O P2 Rh
SMILES	[Rh]([P](c1ccc(cc1)F)(c1ccc(cc1)F)c1ccc(cc1)F)([P](c1ccc(cc1)F)(c1ccc(cc1)F)c1ccc(cc1)F)(Cl)C#[O]
Title of publication	A new polymorph of <i>trans</i>-carbonylchlorobis[tris(4-fluorophenyl)phosphine]rhodium(I)
Authors of publication	Meijboom, Reinout; Muller, Alfred; Roodt, Andreas
Journal of publication	Acta Crystallographica Section E
Year of publication	2006
Journal volume	62
Journal issue	6
Pages of publication	m1309 - m1311
a	11.053 ± 0.0004 Å
b	12.056 ± 0.0004 Å
c	26.514 ± 0.0009 Å
α	83.685 ± 0.002°
β	84.15 ± 0.002°
γ	73.725 ± 0.002°
Cell volume	3361.6 ± 0.2 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.0269
Weighted residual factors for all reflections included in the refinement	0.0668
Goodness-of-fit parameter for all reflections included in the refinement	1.014
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	Yes

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/2209263.html