Information card for entry 2209556

Structure parameters

• Common name: Tetralithiumtetraimidosilicate
• Chemical name: bis(diethyl ether-κO)tetra(tetrahydrofuran-κO)[μ~4~-tetrakis(1- naphthylimido)silane(4-)]tetralithium(I) diethyl ether solvate
• Formula: C68 H90 Li4 N4 O7 Si
• Calculated formula: C68 H90 Li4 N4 O7 Si
• Title of publication: The tetralithium derivative of the tetrakis(1-naphthylimido)silicate tetraanion
• Authors of publication: Copsey, May C.; Balakrishna, Maravanji S.; Chivers, Tristram
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2006
• Journal volume: 62
• Journal issue: 7
• Pages of publication: m1680 - m1682
• a: 27.561 ± 0.006 Å
• b: 14.829 ± 0.003 Å
• c: 17.617 ± 0.004 Å
• α: 90°
• β: 118.38 ± 0.03°
• γ: 90°
• Cell volume: 6335 ± 3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0663
• Residual factor for significantly intense reflections: 0.046
• Weighted residual factors for significantly intense reflections: 0.1134
• Weighted residual factors for all reflections included in the refinement: 0.1275
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes