Information card for entry 2210018

Structure parameters

• Chemical name: Iodotris(triphenylphosphine)nickel(I) diethyl ether hemisolvate
• Formula: C56 H50 I Ni O0.5 P3
• Calculated formula: C56 H50 I Ni O0.5 P3
• Title of publication: Iodotris(triphenylphosphine)nickel(I) diethyl ether hemisolvate
• Authors of publication: Eckert, Nathan A.; Riordan, Charles G.; Yap, Glenn P. A.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2006
• Journal volume: 62
• Journal issue: 8
• Pages of publication: m1766 - m1767
• a: 13.072 ± 0.004 Å
• b: 20.035 ± 0.005 Å
• c: 21.364 ± 0.006 Å
• α: 113.354 ± 0.004°
• β: 105.597 ± 0.004°
• γ: 98.451 ± 0.004°
• Cell volume: 4740 ± 2 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0461
• Residual factor for significantly intense reflections: 0.0354
• Weighted residual factors for significantly intense reflections: 0.079
• Weighted residual factors for all reflections included in the refinement: 0.084
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes