Crystallography Open Database

Information card for entry 2210236

Preview

Structure parameters

Chemical name	<i>cis</i>-Diazido[bis(diphenylphosphino)methane-κ~2~P,P']ruthenium(II) dichloromethane 0.42-solvate
Formula	C50.42 H44.83 Cl0.83 N6 P4 Ru
Calculated formula	C50.417 H44.834 Cl0.834 N6 P4 Ru
Title of publication	<i>cis</i>-Diazido[bis(diphenylphosphino)methane-κ^2^<i>P</i>,<i>P</i>']ruthenium(II) dichloromethane 0.42-solvate
Authors of publication	Luca Russo; Kalle Nättinen; Viatcheslav Vertlib; João Rodrigues; Kari Rissanen
Journal of publication	Acta Crystallographica Section E
Year of publication	2006
Journal volume	62
Journal issue	9
Pages of publication	m2052 - m2053
a	36.8818 ± 0.0007 Å
b	11.2016 ± 0.0002 Å
c	22.3275 ± 0.0004 Å
α	90°
β	97.235 ± 0.002°
γ	90°
Cell volume	9150.8 ± 0.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0856
Residual factor for significantly intense reflections	0.062
Weighted residual factors for significantly intense reflections	0.1482
Weighted residual factors for all reflections included in the refinement	0.1624
Goodness-of-fit parameter for all reflections included in the refinement	1.055
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	Yes

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/2210236.html