Information card for entry 2212637

Structure parameters

• Chemical name: 2-[(2R,3S,4S,5S)-3,4-Benzyloxy-2,5-bis-trityloxymethyl-tetrahydrofuran-2- yloxy]-3,4,5-tribenzyloxy-6-(trityloxymethyl)tetrahydropyran‒methanol‒ 2-butanone (1/1/0.75)
• Formula: C108 H104 O12.75
• Calculated formula: C108.001 H104.004 O12.751
• Title of publication: 2-[(2<i>R</i>,3<i>S</i>,4<i>S</i>,5<i>S</i>)-3,4-Benzyloxy-2,5-bis(trityloxymethyl)tetrahydrofuran-2-yloxy]-3,4,5-tribenzyloxy-6-(trityloxymethyl)tetrahydropyran‒methanol‒2-butanone (1/1/0.75)
• Authors of publication: Zi-Sheng Wu; Chong-Bo Liu; Zhi-Jie Fang; Yuan-Xing Wang; Hui-Liang Wen
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 3
• Pages of publication: o1471 - o1472
• a: 12.9897 ± 0.001 Å
• b: 24.0016 ± 0.0015 Å
• c: 15.9688 ± 0.0011 Å
• α: 90°
• β: 112.322 ± 0.002°
• γ: 90°
• Cell volume: 4605.6 ± 0.6 ų
• Cell temperature: 113 ± 2 K
• Ambient diffraction temperature: 113 ± 2 K
• Number of distinct elements: 3
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0641
• Residual factor for significantly intense reflections: 0.057
• Weighted residual factors for significantly intense reflections: 0.1624
• Weighted residual factors for all reflections included in the refinement: 0.169
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes