Information card for entry 2213396

Structure parameters

• Chemical name: (1-Formyl-2-naphtholato-κ^2^O,O')dioxo(1,10-phenanthroline- κ^2^N,N')vanadium(V) dichloromethane quatersolvate
• Formula: C23.25 H15.5 Cl0.5 N2 O4 V
• Calculated formula: C23.25 H15.5 Cl0.5 N2 O4 V
• Title of publication: (1-Formyl-2-naphtholato-κ^2^<i>O</i>,<i>O</i>')dioxo(1,10-phenanthroline-κ^2^<i>N</i>,<i>N</i>')vanadium(V) dichloromethane 0.25-solvate
• Authors of publication: Jian-Fang Dong; Lian-Zhi Li; Hui Cui; Da-Qi Wang; Tao Xu
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 5
• Pages of publication: m1458 - m1460
• a: 13.86 ± 0.002 Å
• b: 7.3946 ± 0.0014 Å
• c: 21.063 ± 0.002 Å
• α: 90°
• β: 90.105 ± 0.002°
• γ: 90°
• Cell volume: 2158.7 ± 0.6 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1679
• Residual factor for significantly intense reflections: 0.0929
• Weighted residual factors for significantly intense reflections: 0.237
• Weighted residual factors for all reflections included in the refinement: 0.3023
• Goodness-of-fit parameter for all reflections included in the refinement: 0.979
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes