Information card for entry 2213436

Structure parameters

• Chemical name: Di-μ-thiocyanato-κ^2^S:N;κ^2^N:S-bis{[N,N-dimethyl-N'-(2-pyridylmethylene- κN)ethane-1,2-diamine-κ^2^N,N']nickel(II)} bis(perchlorate)
• Formula: C22 H30 Cl2 N8 Ni2 O8 S2
• Calculated formula: C22 H30 Cl2 N8 Ni2 O8 S2
• Title of publication: Di-μ-thiocyanato-κ^2^<i>S</i>:<i>N</i>;κ^2^<i>N</i>:<i>S</i>-bis{[<i>N</i>,<i>N</i>-dimethyl-<i>N</i>'-(2-pyridylmethylene-κ<i>N</i>)ethane-1,2-diamine-κ^2^<i>N</i>,<i>N</i>']nickel(II)} bis(perchlorate)
• Authors of publication: Yun-Peng Diao
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 5
• Pages of publication: m1453 - m1454
• a: 6.348 ± 0.001 Å
• b: 24.834 ± 0.003 Å
• c: 10.134 ± 0.001 Å
• α: 90°
• β: 98.442 ± 0.002°
• γ: 90°
• Cell volume: 1580.3 ± 0.4 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1018
• Residual factor for significantly intense reflections: 0.0779
• Weighted residual factors for significantly intense reflections: 0.1932
• Weighted residual factors for all reflections included in the refinement: 0.215
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes