Information card for entry 2214274

Structure parameters

• Chemical name: Chlorido(1-pyrrolidinecarbodithioato-κ^2^S,S')(triphenylphosphine- κP)nickel(II) chloroform hemisolvate
• Formula: C47 H47 Cl5 N2 Ni2 P2 S4
• Calculated formula: C47 H47 Cl5 N2 Ni2 P2 S4
• Title of publication: Chlorido(1-pyrrolidinecarbodithioato-κ^2^<i>S</i>,<i>S</i>')(triphenylphosphine-κ<i>P</i>)nickel(II) chloroform hemisolvate
• Authors of publication: Kropidłowska, Anna; Janczak, Jan; Gołaszewska, Jolanta; Becker, Barbara
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 7
• Pages of publication: m1947 - m1947
• a: 9.713 ± 0.002 Å
• b: 10.076 ± 0.002 Å
• c: 14.509 ± 0.003 Å
• α: 90.37 ± 0.02°
• β: 91.21 ± 0.02°
• γ: 117.39 ± 0.02°
• Cell volume: 1260.3 ± 0.5 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1597
• Residual factor for significantly intense reflections: 0.0577
• Weighted residual factors for significantly intense reflections: 0.1072
• Weighted residual factors for all reflections included in the refinement: 0.119
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes