Information card for entry 2214529

Structure parameters

• Chemical name: catena-Poly[[tetrakis(hexamethylphosphoramide-κO)bis(nitrato- κ^2^O,O')ytterbium(III)] [silver(I)-di-μ-sulfido-tungstate(VI)(Ag—W)-di-μ-sulfido]]
• Formula: C24 H72 Ag N14 O10 P4 S4 W Yb
• Calculated formula: C24 H72 Ag N14 O10 P4 S4 W Yb
• SMILES: [Yb]12([O]=P(N(C)C)(N(C)C)N(C)C)([O]=P(N(C)C)(N(C)C)N(C)C)([O]=P(N(C)C)(N(C)C)N(C)C)([O]=P(N(C)C)(N(C)C)N(C)C)([O]=N(=O)O1)[O]=N(=O)O2.[Yb]12([O]=P(N(C)C)(N(C)C)N(C)C)([O]=P(N(C)C)(N(C)C)N(C)C)([O]=P(N(C)C)(N(C)C)N(C)C)([O]=P(N(C)C)(N(C)C)N(C)C)([O]=N(=O)O1)[O]=N(=O)O2.[Ag]1S[W](S1)(=[S]2)=[S][Ag]21S[W](S1)(=S)=S
• Title of publication: <i>catena</i>-Poly[[tetrakis(hexamethylphosphoramide-κ<i>O</i>)bis(nitrato- κ^2^<i>O</i>,<i>O</i>')ytterbium(III)] [silver(I)-di-μ-sulfido-tungstate(VI)(<i>Ag</i>—<i>W</i>)-di-μ-sulfido]]
• Authors of publication: Cao, Yuan; Zhang, Jin-Fang; Zhang, Chi
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 8
• Pages of publication: m2076 - m2077
• a: 15.7241 ± 0.0009 Å
• b: 29.528 ± 0.0018 Å
• c: 11.3464 ± 0.0007 Å
• α: 90°
• β: 90.798 ± 0.001°
• γ: 90°
• Cell volume: 5267.6 ± 0.5 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0354
• Residual factor for significantly intense reflections: 0.0325
• Weighted residual factors for significantly intense reflections: 0.0674
• Weighted residual factors for all reflections included in the refinement: 0.0686
• Goodness-of-fit parameter for all reflections included in the refinement: 1.179
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes