Information card for entry 2216268

Structure parameters

• Chemical name: Bis{μ-1,4-bis[(diphenylphosphanyl)ethynyl]benzene-κ^2^P:P'}bis[trans- diiodidopalladium(II)] chloroform trisolvate
• Formula: C71 H51 Cl9 I4 P4 Pd2
• Calculated formula: C71 H51 Cl9 I4 P4 Pd2
• Title of publication: Bis{μ-1,4-bis[(diphenylphosphanyl)ethynyl]benzene-κ^2^<i>P</i>:<i>P</i>'}bis[<i>trans</i>-diiodidopalladium(II)] chloroform trisolvate
• Authors of publication: Chan, Wing Yan; Baumgartner, Thomas; Lough, Alan J.; Manners, Ian
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 12
• Pages of publication: m2886 - m2886
• a: 20.896 ± 0.0009 Å
• b: 9.592 ± 0.0005 Å
• c: 38.832 ± 0.002 Å
• α: 90°
• β: 99.804 ± 0.003°
• γ: 90°
• Cell volume: 7669.6 ± 0.7 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1302
• Residual factor for significantly intense reflections: 0.0555
• Weighted residual factors for significantly intense reflections: 0.0888
• Weighted residual factors for all reflections included in the refinement: 0.1118
• Goodness-of-fit parameter for all reflections included in the refinement: 1.007
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes