Information card for entry 2217333

Structure parameters

• Chemical name: Bis[1,2-bis(dimethylphosphino)ethane]dichloridonitrosyltungsten(0) chloride
• Formula: C12 H32 Cl3 N O P4 W
• Calculated formula: C12 H32 Cl3 N O P4 W
• Title of publication: Bis[1,2-bis(dimethylphosphino)ethane]dichloridonitrosyltungsten(0) chloride
• Authors of publication: Avramović, Nataša; Blacque, Olivier; Schmalle, Helmut W.; Berke, Heinz
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 1
• Pages of publication: m245 - m245
• a: 8.0929 ± 0.0007 Å
• b: 26.118 ± 0.002 Å
• c: 10.5703 ± 0.001 Å
• α: 90°
• β: 94.19 ± 0.01°
• γ: 90°
• Cell volume: 2228.3 ± 0.3 ų
• Cell temperature: 183 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0317
• Residual factor for significantly intense reflections: 0.0249
• Weighted residual factors for significantly intense reflections: 0.0581
• Weighted residual factors for all reflections included in the refinement: 0.0597
• Goodness-of-fit parameter for all reflections included in the refinement: 0.975
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes