Information card for entry 2217499

Structure parameters

• Chemical name: Bis[μ-1,2-bis(diphenylphosphino)methane-κ^2^<i>P</i>:<i>P</i>']bis[(η^2^- ethene)nickel(0)] toluene disolvate
• Formula: C68 H68 Ni2 P4
• Calculated formula: C68 H68 Ni2 P4
• Title of publication: Bis[μ-1,2-bis(diphenylphosphino)methane-κ^2^<i>P</i>:<i>P</i>']bis[(η^2^-ethene)nickel(0)] toluene disolvate
• Authors of publication: Langer, Jens; Fischer, Reinhald; Görls, Helmar; Walther, Dirk
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 2
• Pages of publication: m412 - m412
• a: 13.0963 ± 0.0012 Å
• b: 15.2367 ± 0.0016 Å
• c: 15.6177 ± 0.0016 Å
• α: 70.566 ± 0.004°
• β: 78.727 ± 0.004°
• γ: 78.689 ± 0.007°
• Cell volume: 2853.1 ± 0.5 ų
• Cell temperature: 183 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1256
• Residual factor for significantly intense reflections: 0.0857
• Weighted residual factors for significantly intense reflections: 0.2072
• Weighted residual factors for all reflections included in the refinement: 0.2331
• Goodness-of-fit parameter for all reflections included in the refinement: 1.135
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes