Information card for entry 2217561

Structure parameters

• Chemical name: <i>catena</i>-Poly[[[<i>trans</i>-diaquabis(pyridine-κN)cobalt(II)]- μ-(4-{N'-[1-(3-acetyl-4-methyl-1<i>H</i>-pyrazol-5- yl)ethylidene]hydrazino}benzoato-κ^3^<i>O</i>:<i>N</i>,<i>N</i>')- [bis(pyridine-κN)cobalt(III)]-μ-(4-{N'-[1-(3-acetyl-4-methyl-1<i>H</i>- pyrazol-5-yl)ethylidene]hydrazino}benzoato- κ^3^<i>N</i>,<i>N'</i>:<i>O</i>)]perchlorate 3.66-hydrate]
• Formula: C50 H59.33 Cl Co2 N12 O15.66
• Calculated formula: C50 H56 Cl Co2 N12 O15.66
• Title of publication: <i>catena</i>-Poly[[[<i>trans</i>-diaquabis(pyridine-κ<i>N</i>)cobalt(II)]-μ-(4-{<i>N</i>'-[1-(3-acetyl-4-methyl-1<i>H</i>-pyrazol-5-yl)ethylidene]hydrazino}benzoato-κ^3^<i>O</i>:<i>N</i>,<i>N</i>')-[bis(pyridine-κ<i>N</i>)cobalt(III)]-μ-(4-{<i>N</i>'-[1-(3-acetyl-4-methyl-1<i>H</i>-pyrazol-5-yl)ethylidene]hydrazino}benzoato-κ^3^<i>N</i>,<i>N</i>':<i>O</i>)]perchlorate 3.66-hydrate]
• Authors of publication: Penkova, Larysa; Azarkh, Mikhail P.; Haukka, Matti; Meyer, Franc; Fritsky, Igor O.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 2
• Pages of publication: m432 - m433
• a: 10.1128 ± 0.0002 Å
• b: 13.9615 ± 0.0004 Å
• c: 20.184 ± 0.0006 Å
• α: 85.969 ± 0.002°
• β: 80.844 ± 0.002°
• γ: 84.66 ± 0.002°
• Cell volume: 2796.79 ± 0.13 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0705
• Residual factor for significantly intense reflections: 0.0458
• Weighted residual factors for significantly intense reflections: 0.1127
• Weighted residual factors for all reflections included in the refinement: 0.1247
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes