Information card for entry 2217619

Structure parameters

• Chemical name: (μ-5-Carboxybenzene-1,3-dicarboxylato-κ^2^O^1^:O^3^)bis[bis(2,2'-bipyridine- κ^2^<i>N</i>,<i>N</i>')copper(II)] 5-carboxybenzene-1,3-dicarboxylate 2,2'-bipyridine solvate tridecahydrate
• Formula: C68 H74 Cu2 N10 O25
• Calculated formula: C68 H70.5 Cu2 N10 O25
• Title of publication: (μ-5-Carboxybenzene-1,3-dicarboxylato-κ^2^<i>O</i>^1^:<i>O</i>^3^)bis[bis(2,2'-bipyridine-κ^2^<i>N</i>,<i>N</i>')copper(II)] 5-carboxybenzene-1,3-dicarboxylate 2,2'-bipyridine solvate tridecahydrate
• Authors of publication: Marek, Jaromír; Trávníček, Zdeněk
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 2
• Pages of publication: m384 - m385
• a: 14.4638 ± 0.0002 Å
• b: 19.7448 ± 0.0002 Å
• c: 25.0638 ± 0.0003 Å
• α: 90°
• β: 99.2051 ± 0.0014°
• γ: 90°
• Cell volume: 7065.66 ± 0.15 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0419
• Residual factor for significantly intense reflections: 0.0343
• Weighted residual factors for significantly intense reflections: 0.0813
• Weighted residual factors for all reflections included in the refinement: 0.0855
• Goodness-of-fit parameter for all reflections included in the refinement: 0.987
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes