Information card for entry 2217894

Structure parameters

• Chemical name: Poly[[aqua-μ~3~-picolinato-μ~2~-picolinato- dipicolinatopotassium(I)terbium(III)] 2.5-hydrate]
• Formula: C24 H23 K N4 O11.5 Tb
• Calculated formula: C24 H23 K N4 O11.5 Tb
• Title of publication: Poly[[aqua-μ~3~-picolinato-μ~2~-picolinato-dipicolinatopotassium(I)terbium(III)] 2.5-hydrate]
• Authors of publication: Cunha-Silva, Luís; Soares-Santos, Paula C. R.; Nogueira, Helena I. S.; Trindade, Tito; Klinowski, Jacek; Rocha, João; Almeida Paz, Filipe A.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 4
• Pages of publication: m529 - m530
• a: 12.7187 ± 0.0002 Å
• b: 12.7187 ± 0.0002 Å
• c: 62.2321 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 8718.3 ± 0.2 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 179
• Hermann-Mauguin space group symbol: P 65 2 2
• Hall space group symbol: P 65 2 (0 0 1)
• Residual factor for all reflections: 0.0397
• Residual factor for significantly intense reflections: 0.0324
• Weighted residual factors for significantly intense reflections: 0.0908
• Weighted residual factors for all reflections included in the refinement: 0.0943
• Goodness-of-fit parameter for all reflections included in the refinement: 1.138
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes