Information card for entry 2218058

Structure parameters

• Chemical name: [1,2-Bis(diphenylphosphino)ethane]{2- [bis(diphenylphosphinomethyl)amino]pyridinium}fluoridohydrazidatomolybdenum(IV) bis(tetrafluoridoborate)
• Formula: C57 H55 B2 F9 Mo N4 P4
• Calculated formula: C57 H55 B2 F9 Mo N4 P4
• Title of publication: [1,2-Bis(diphenylphosphino)ethane]{2-[bis(diphenylphosphinomethyl)amino]pyridinium}fluoridohydrazidatomolybdenum(IV) bis(tetrafluoridoborate)
• Authors of publication: Stephan, Gerald; Näther, Christian; Tuczek, Felix
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 5
• Pages of publication: m629
• a: 12.5791 ± 0.0006 Å
• b: 31.2199 ± 0.0016 Å
• c: 13.833 ± 0.0009 Å
• α: 90°
• β: 94.438 ± 0.007°
• γ: 90°
• Cell volume: 5416.2 ± 0.5 ų
• Cell temperature: 170 ± 2 K
• Ambient diffraction temperature: 170 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.053
• Residual factor for significantly intense reflections: 0.0394
• Weighted residual factors for significantly intense reflections: 0.1016
• Weighted residual factors for all reflections included in the refinement: 0.1077
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes