Information card for entry 2218073

Structure parameters

• Chemical name: μ-4,4'-bipyridyl-1:2κ^2^<i>N</i>:<i>N</i>'-methanol-2κO-tetrakis(tri- <i>tert</i>-butoxysilanethiolato)-1κ^4^O,S;2κ^2^S-dizinc(II)
• Formula: C59 H120 N2 O13 S4 Si4 Zn2
• Calculated formula: C59 H120 N2 O13 S4 Si4 Zn2
• Title of publication: μ-4,4'-Bipyridyl-1:2κ^2^<i>N</i>:<i>N</i>'-methanol-2κ<i>O</i>-tetrakis(tri-<i>tert</i>-butoxysilanethiolato)-1κ^4^<i>O</i>,<i>S</i>;2κ^2^<i>S</i>-dizinc(II)
• Authors of publication: Dołega, Anna; Baranowska, Katarzyna
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 5
• Pages of publication: m616 - m617
• a: 9.5897 ± 0.0002 Å
• b: 36.8378 ± 0.0011 Å
• c: 22.7611 ± 0.0005 Å
• α: 90°
• β: 99.127 ± 0.002°
• γ: 90°
• Cell volume: 7938.9 ± 0.3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 7
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0536
• Residual factor for significantly intense reflections: 0.044
• Weighted residual factors for significantly intense reflections: 0.1206
• Weighted residual factors for all reflections included in the refinement: 0.1258
• Goodness-of-fit parameter for all reflections included in the refinement: 1.185
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes