Information card for entry 2218106

Structure parameters

• Chemical name: Bis[(2-pyridylmethyl)(triisopropylsilyl)amido]zinc(II)‒ toluene‒tetrahydrofuran (4/2/1)
• Formula: C34.5 H60 N4 O0.25 Si2 Zn
• Calculated formula: C34.5 H60 N4 O0.25 Si2 Zn
• Title of publication: Bis[(2-pyridylmethyl)(triisopropylsilyl)amido]zinc(II)‒toluene‒tetrahydrofuran (4/2/1)
• Authors of publication: Koch, Christian; Görls, Helmar; Westerhausen, Matthias
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 5
• Pages of publication: m664
• a: 13.241 ± 0.0003 Å
• b: 17.6223 ± 0.0004 Å
• c: 16.7978 ± 0.0005 Å
• α: 90°
• β: 91.018 ± 0.002°
• γ: 90°
• Cell volume: 3918.93 ± 0.17 ų
• Cell temperature: 183 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0982
• Residual factor for significantly intense reflections: 0.0611
• Weighted residual factors for significantly intense reflections: 0.1525
• Weighted residual factors for all reflections included in the refinement: 0.1732
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes