Information card for entry 2218187

Structure parameters

• Chemical name: Tetrakis(μ~3~-2-{[1,1-bis(hydroxymethyl)-2-oxidoethyl]iminomethyl}- 6-methoxyphenolato)tetranickel(II) tetrahydrate
• Formula: C48 H68 N4 Ni4 O24
• Calculated formula: C48 H68 N4 Ni4 O24
• Title of publication: Tetrakis(μ~3~-2-{[1,1-bis(hydroxymethyl)-2-oxidoethyl]iminomethyl}-6-methoxyphenolato)tetranickel(II) tetrahydrate
• Authors of publication: Guo, Yujing; Li, Lianzhi; Liu, Yan; Dong, Jianfang; Wang, Daqi
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 5
• Pages of publication: m675 - m676
• a: 18.754 ± 0.002 Å
• b: 18.754 ± 0.002 Å
• c: 15.4395 ± 0.0015 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5430.3 ± 1 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 88
• Hermann-Mauguin space group symbol: I 41/a :2
• Hall space group symbol: -I 4ad
• Residual factor for all reflections: 0.088
• Residual factor for significantly intense reflections: 0.0655
• Weighted residual factors for significantly intense reflections: 0.1694
• Weighted residual factors for all reflections included in the refinement: 0.194
• Goodness-of-fit parameter for all reflections included in the refinement: 1.076
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes