Information card for entry 2218319

Structure parameters

• Chemical name: (2-Hydroxyphenylimido-κN)(methanolato-κO)[2-(2- oxidobenzylideneamino)phenolato- κ^2^O,N,O'](triphenylphosphine-κP)rhenium(V)
• Formula: C38 H32 N2 O4 P Re
• Calculated formula: C38 H32 N2 O4 P Re
• Title of publication: (2-Hydroxyphenylimido-κ<i>N</i>)(methanolato-κ<i>O</i>)[2-(2-oxidobenzylideneamino)phenolato-κ^2^<i>O</i>,<i>N</i>,<i>O</i>'](triphenylphosphine-κ<i>P</i>)rhenium(V)
• Authors of publication: Holland, Jason P.; Barnard, Peter J.; Dilworth, Jonathan R.; Watkin, David J.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 6
• Pages of publication: m773
• a: 10.0193 ± 0.0002 Å
• b: 32.9759 ± 0.0003 Å
• c: 19.4605 ± 0.0002 Å
• α: 90°
• β: 90.1597 ± 0.0004°
• γ: 90°
• Cell volume: 6429.64 ± 0.16 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0674
• Residual factor for significantly intense reflections: 0.0457
• Weighted residual factors for all reflections: 0.0852
• Weighted residual factors for significantly intense reflections: 0.0788
• Weighted residual factors for all reflections included in the refinement: 0.0851
• Goodness-of-fit parameter for all reflections included in the refinement: 0.9892
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes