Information card for entry 2218527

Structure parameters

• Chemical name: [η^5^-2,3-Bis(trimethylsilyl)-2,3-dicarba-<i>nido</i>- hexaborane(2-)]chlorido(N,N,N',N'-tetramethylethylenediamine)dysprosium(III)
• Formula: C28 H76 B8 Cl2 Dy2 N4 Si4
• Calculated formula: C28 H76 B8 Cl2 Dy2 N4 Si4
• SMILES: [B]12345[BH]678[BH]9%101[C]12([C]29([Dy]9%11%12361(Cl)([N](CC[N]%12(C)C)(C)C)([BH]7%102)[BH]123[B]679([BH]9%102[BH]21[C]1%10([C]69([Dy]6583721([H]4)(Cl)[N](CC[N]6(C)C)(C)C)[Si](C)(C)C)[Si](C)(C)C)[H]%11)[Si](C)(C)C)[Si](C)(C)C
• Title of publication: [η^5^-2,3-Bis(trimethylsilyl)-2,3-dicarba-<i>nido</i>-hexaborane(2{-})]chlorido(<i>N</i>,<i>N</i>,<i>N</i>',<i>N</i>'-tetramethylethylenediamine)dysprosium(III)
• Authors of publication: Zheng, Chong; Canseco-Melchor, Graciela; Maguire, John A.; Hosmane, Narayan S.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 6
• Pages of publication: m799
• a: 11.4467 ± 0.0008 Å
• b: 14.8624 ± 0.001 Å
• c: 13.8615 ± 0.0009 Å
• α: 90°
• β: 92.77 ± 0.001°
• γ: 90°
• Cell volume: 2355.4 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0237
• Residual factor for significantly intense reflections: 0.0235
• Weighted residual factors for significantly intense reflections: 0.0502
• Weighted residual factors for all reflections included in the refinement: 0.0503
• Goodness-of-fit parameter for all reflections included in the refinement: 1.441
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes