Information card for entry 2218774

Structure parameters

• Chemical name: <i>catena</i>-Poly[[[bis(<i>O</i>,<i>O</i>'-diisobutyl dithiophosphato-κ^2^<i>S</i>,<i>S</i>')nickel(II)]-μ-1,2- bis(4-pyridylmethylene)hydrazine-κ^2^<i>N</i>:<i>N</i>'] toluene disolvate]
• Formula: C42 H62 N4 Ni O4 P2 S4
• Calculated formula: C42 H62 N4 Ni O4 P2 S4
• Title of publication: <i>catena</i>-Poly[[[bis(<i>O</i>,<i>O</i>'-diisobutyl dithiophosphato-κ^2^<i>S</i>,<i>S</i>')nickel(II)]-μ-1,2-bis(4-pyridylmethylene)hydrazine-κ^2^<i>N</i>:<i>N</i>'] toluene disolvate]
• Authors of publication: Berdugo, Erick; Tiekink, Edward R. T.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 7
• Pages of publication: m911
• a: 8.7132 ± 0.0015 Å
• b: 12.089 ± 0.002 Å
• c: 12.293 ± 0.002 Å
• α: 82.662 ± 0.01°
• β: 86.528 ± 0.01°
• γ: 69.321 ± 0.006°
• Cell volume: 1201.4 ± 0.4 ų
• Cell temperature: 98 ± 2 K
• Ambient diffraction temperature: 28 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.059
• Residual factor for significantly intense reflections: 0.054
• Weighted residual factors for significantly intense reflections: 0.138
• Weighted residual factors for all reflections included in the refinement: 0.142
• Goodness-of-fit parameter for all reflections included in the refinement: 1.08
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes