Information card for entry 2219606

Structure parameters

• Chemical name: {Bis[2-(dicyclohexylphosphino)phenyl]methylsilyl- κ^3^<i>P</i>,<i>Si</i>,<i>P</i>'}chloridopalladium(II)
• Formula: C37 H55 Cl P2 Pd Si
• Calculated formula: C37 H55 Cl P2 Pd Si
• SMILES: [Pd]12(Cl)[P](c3c([Si]2(C)c2ccccc2[P]1(C1CCCCC1)C1CCCCC1)cccc3)(C1CCCCC1)C1CCCCC1
• Title of publication: {Bis[2-(dicyclohexylphosphino)phenyl]methylsilyl-κ^3^<i>P</i>,<i>Si</i>,<i>P</i>'}chloridopalladium(II)
• Authors of publication: Li, Yong-Hua; Zhang, Yuan; Zhao, Min-Min; Yuan, Yu-Yu
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 10
• Pages of publication: m1271
• a: 13.079 ± 0.003 Å
• b: 16.632 ± 0.003 Å
• c: 17.739 ± 0.004 Å
• α: 90°
• β: 108.55 ± 0.03°
• γ: 90°
• Cell volume: 3658.3 ± 1.5 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0341
• Residual factor for significantly intense reflections: 0.0258
• Weighted residual factors for significantly intense reflections: 0.0581
• Weighted residual factors for all reflections included in the refinement: 0.0591
• Goodness-of-fit parameter for all reflections included in the refinement: 0.928
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes