Information card for entry 2219919

Structure parameters

• Chemical name: Di-μ-chlorido-2:3κ^4^Cl:Cl-dichlorido-1κCl,4κCl-bis{μ-6,6'-dimethoxy- 2,2'-[o-phenylenebis(nitrilomethylidyne)]diphenolato}- 1:2κ^4^N,N',O^1^,O^1'^:κ^4^O^1^,O^1'^,O^6^,O^6'^; 3:4κ^4^O^1^,O^1'^,O^6^,O^6'^:κ^4^N,N',O^1^,O^1'^-2,3-dilead(II)-1,4-dizinc(II) <i>N</i>,<i>N'</i>-dimethylformamide disolvate
• Formula: C50 H50 Cl4 N6 O10 Pb2 Zn2
• Calculated formula: C50 H50 Cl4 N6 O10 Pb2 Zn2
• SMILES: COc1cccc2c1[O]1[Pb](Cl)[O]3[Zn]41([N](=C2)c1c([N]4=Cc2c3c(OC)ccc2)cccc1)Cl.O=CN(C)C
• Title of publication: Di-μ-chlorido-dichlorido-bis{μ-6,6'-dimethoxy-2,2'-[<i>o</i>-phenylenebis(nitrilomethylidyne)]diphenolato}dilead(II)dizinc(II) <i>N</i>,<i>N</i>'-dimethylformamide disolvate
• Authors of publication: Wang, Hailong; Zhang, Daopeng; Zhang, Li-Fang
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 11
• Pages of publication: m1408 - m1409
• a: 7.4955 ± 0.0006 Å
• b: 32.119 ± 0.003 Å
• c: 11.2366 ± 0.0009 Å
• α: 90°
• β: 95.729 ± 0.002°
• γ: 90°
• Cell volume: 2691.7 ± 0.4 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.076
• Residual factor for significantly intense reflections: 0.0378
• Weighted residual factors for significantly intense reflections: 0.0581
• Weighted residual factors for all reflections included in the refinement: 0.0658
• Goodness-of-fit parameter for all reflections included in the refinement: 0.932
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes