Crystallography Open Database

Information card for entry 2220067

2220066 << 2220067 >> 2220068

Preview

Structure parameters

Chemical name	4-Desoxy-4β-[(5-methoxy-1H-indol-3-yl)oxalylamino]podophyllotoxin methanol solvate
Formula	C34 H34 N2 O11
Calculated formula	C34 H34 N2 O11
Title of publication	4-Desoxy-4β-[(5-methoxy-1<i>H</i>-indol-3-yl)oxalylamino]podophyllotoxin methanol solvate
Authors of publication	Feng, Min; Zhao, Ming; Zhang, Jingze; Yang, Zaixin; Chen, Hong
Journal of publication	Acta Crystallographica Section E
Year of publication	2008
Journal volume	64
Journal issue	12
Pages of publication	o2339
a	12.228 ± 0.002 Å
b	9.836 ± 0.0016 Å
c	26.667 ± 0.005 Å
α	90°
β	95.58 ± 0.03°
γ	90°
Cell volume	3192.2 ± 1 Å³
Cell temperature	113 ± 2 K
Ambient diffraction temperature	113 ± 2 K
Number of distinct elements	4
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.054
Residual factor for significantly intense reflections	0.047
Weighted residual factors for significantly intense reflections	0.1207
Weighted residual factors for all reflections included in the refinement	0.1265
Goodness-of-fit parameter for all reflections included in the refinement	1.032
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	Yes

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/2220067.html