Information card for entry 2220117

Structure parameters

• Chemical name: Di-μ1,1-azido-bis[azido(5,5'-dimethyl-2,2'-bipyridine)nickel(II)]
• Formula: C24 H24 N16 Ni2
• Calculated formula: C24 H24 N16 Ni2
• SMILES: c12ccc(c[n]2[Ni]2(N=N#N)([n]3c1ccc(c3)C)[N](=N#N)[Ni]1([n]3c(ccc(c3)C)c3ccc(c[n]13)C)(N=N#N)[N]2=N#N)C
• Title of publication: Di-μ~1,1~-azido-bis[azido(5,5'-dimethyl-2,2'-bipyridine)nickel(II)]
• Authors of publication: Hou, Jin
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 12
• Pages of publication: m1571
• a: 7.938 ± 0.002 Å
• b: 15.067 ± 0.003 Å
• c: 11.755 ± 0.002 Å
• α: 90°
• β: 91.65 ± 0.002°
• γ: 90°
• Cell volume: 1405.3 ± 0.5 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0857
• Residual factor for significantly intense reflections: 0.0562
• Weighted residual factors for significantly intense reflections: 0.1355
• Weighted residual factors for all reflections included in the refinement: 0.1493
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes