Information card for entry 2220244

Structure parameters

• Chemical name: di-μ-oxido-bis({2-[2-(methylamino)ethyliminomethyl]phenolato- κ^3^N,N',O}oxidovanadium(V))
• Formula: C20 H26 N4 O6 V2
• Calculated formula: C20 H26 N4 O6 V2
• Title of publication: A monoclinic polymorph of di-μ-oxido-bis({2-[2-(methylamino)ethyliminomethyl]phenolato-κ^3^<i>N</i>,<i>N</i>',<i>O</i>}oxidovanadium(V))
• Authors of publication: Romanowski, Grzegorz; Wera, Michał; Sikorski, Artur
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 12
• Pages of publication: m1548 - m1549
• a: 6.6801 ± 0.0002 Å
• b: 11.9955 ± 0.0006 Å
• c: 13.8643 ± 0.0007 Å
• α: 90°
• β: 92.156 ± 0.004°
• γ: 90°
• Cell volume: 1110.18 ± 0.09 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0677
• Residual factor for significantly intense reflections: 0.0438
• Weighted residual factors for significantly intense reflections: 0.1
• Weighted residual factors for all reflections included in the refinement: 0.106
• Goodness-of-fit parameter for all reflections included in the refinement: 0.896
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes