Information card for entry 2221231

Structure parameters

• Chemical name: 1,2-Dihydrospiro[carbazole-3(4<i>H</i>),2'-[1,3]dioxolane]
• Formula: C14 H15 N O2
• Calculated formula: C14 H15 N O2
• SMILES: O1C2(OCC1)Cc1c3c([nH]c1CC2)cccc3
• Title of publication: 1,2-Dihydrospiro[carbazole-3(4<i>H</i>),2'-[1,3]dioxolane]
• Authors of publication: Bjerrum, Janni Vester; Ulven, Trond; Bond, Andrew D.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2009
• Journal volume: 65
• Journal issue: 3
• Pages of publication: o579
• a: 9.3781 ± 0.0006 Å
• b: 6.1467 ± 0.0004 Å
• c: 10.574 ± 0.0007 Å
• α: 90°
• β: 115.232 ± 0.002°
• γ: 90°
• Cell volume: 551.38 ± 0.06 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 4
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.03
• Residual factor for significantly intense reflections: 0.029
• Weighted residual factors for significantly intense reflections: 0.079
• Weighted residual factors for all reflections included in the refinement: 0.08
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes