Information card for entry 2221289

Structure parameters

• Chemical name: <i>trans</i>-Di-μ-acetato-[μ-<i>N</i>,<i>N</i>- bis(diphenylphosphino)aniline]bis[chloridomolybdenum(II)](<i>Mo—Mo</i>)‒ dichloromethane‒tetrahydrofuran (1/0.3/1.7)
• Formula: C41.1 H45.2 Cl2.6 Mo2 N O5.7 P2
• Calculated formula: C41.1 H45.2 Cl2.6 Mo2 N O5.7 P2
• Title of publication: <i>trans</i>-Di-μ-acetato-[μ-<i>N</i>,<i>N</i>-bis(diphenylphosphino)aniline]bis[chloridomolybdenum(II)](<i>Mo{—</i>Mo})‒dichloromethane‒tetrahydrofuran (1/0.3/1.7)
• Authors of publication: Hapke, Marko; Wöhl, Anina; Peitz, Stephan; Spannenberg, Anke; Rosenthal, Uwe
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2009
• Journal volume: 65
• Journal issue: 4
• Pages of publication: m357
• a: 15.769 ± 0.003 Å
• b: 13.913 ± 0.003 Å
• c: 20.108 ± 0.004 Å
• α: 90°
• β: 107.32 ± 0.03°
• γ: 90°
• Cell volume: 4211.5 ± 1.6 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0519
• Residual factor for significantly intense reflections: 0.0332
• Weighted residual factors for significantly intense reflections: 0.0722
• Weighted residual factors for all reflections included in the refinement: 0.0759
• Goodness-of-fit parameter for all reflections included in the refinement: 0.904
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes