Information card for entry 2221490

Structure parameters

• Chemical name: Poly[bis(methanol-κ<i>O</i>)tris(μ-pyrimidine- κ^2^<i>N</i>:<i>N</i>')tetrakis(thiocyanato-κ<i>N</i>)dinickel(II)]
• Formula: C18 H20 N10 Ni2 O2 S4
• Calculated formula: C18 H20 N10 Ni2 O2 S4
• Title of publication: Poly[bis(methanol-κ<i>O</i>)tris(μ-pyrimidine-κ^2^<i>N</i>:<i>N</i>')tetrakis(thiocyanato-κ<i>N</i>)dinickel(II)]
• Authors of publication: Wriedt, Mario; Sellmer, Sina; Jess, Inke; Näther, Christian
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2009
• Journal volume: 65
• Journal issue: 4
• Pages of publication: m361 - m362
• a: 20.0624 ± 0.0004 Å
• b: 32.5018 ± 0.0006 Å
• c: 8.0268 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5233.99 ± 0.19 ų
• Cell temperature: 80 ± 2 K
• Ambient diffraction temperature: 80 ± 2 K
• Number of distinct elements: 6
• Space group number: 43
• Hermann-Mauguin space group symbol: F d d 2
• Hall space group symbol: F 2 -2d
• Residual factor for all reflections: 0.0208
• Residual factor for significantly intense reflections: 0.0199
• Weighted residual factors for significantly intense reflections: 0.0479
• Weighted residual factors for all reflections included in the refinement: 0.0482
• Goodness-of-fit parameter for all reflections included in the refinement: 1.088
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes