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Information card for entry 2221646
Preview
Coordinates | 2221646.cif |
---|---|
Structure factors | 2221646.hkl |
Original IUCr paper | HTML |
Chemical name | Bis(2,2'-bipyridyl)-1κ^2^<i>N</i>,<i>N</i>';3κ^2^<i>N</i>,<i>N</i>'- bis(4-bromo-2-formylphenolato)- 1κ^2^<i>O</i>,<i>O</i>';3κ^2^<i>O</i>,<i>O</i>'- bis[μ-2-(5-bromo-2-oxidobenzylideneamino)ethanesulfonato]- 1:2κ^3^<i>O</i>:<i>N</i>,<i>O</i>^2^;2:3κ^3^<i>N</i>,<i>O</i>^2^:<i>O</i>- tricopper(II) monohydrate |
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Formula | C52 H42 Br4 Cu3 N6 O13 S2 |
Calculated formula | C52 H42 Br4 Cu3 N6 O13 S2 |
Title of publication | Bis(2,2'-bipyridyl)-1κ^2^<i>N</i>,<i>N</i>';3κ^2^<i>N</i>,<i>N</i>'-bis(4-bromo-2-formylphenolato)-1κ^2^<i>O</i>,<i>O</i>';3κ^2^<i>O</i>,<i>O</i>'-bis[μ-2-(5-bromo-2-oxidobenzylideneamino)ethanesulfonato]-1:2κ^3^<i>O</i>:<i>N</i>,<i>O</i>^2^;2:3κ^3^<i>N</i>,<i>O</i>^2^:<i>O</i>-tricopper(II) monohydrate |
Authors of publication | Zhang, Ling |
Journal of publication | Acta Crystallographica Section E |
Year of publication | 2009 |
Journal volume | 65 |
Journal issue | 5 |
Pages of publication | m552 |
a | 10.031 ± 0.002 Å |
b | 11.48 ± 0.002 Å |
c | 12.913 ± 0.003 Å |
α | 73.13 ± 0.03° |
β | 78.58 ± 0.03° |
γ | 75.24 ± 0.03° |
Cell volume | 1363.6 ± 0.6 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1763 |
Residual factor for significantly intense reflections | 0.0473 |
Weighted residual factors for significantly intense reflections | 0.0806 |
Weighted residual factors for all reflections included in the refinement | 0.0993 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.758 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | Yes |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/2221646.html
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