Information card for entry 2221846

Structure parameters

• Chemical name: [1,2-Bis(diphenylphosphino)-1,2-dicarba-<i>closo</i>-dodecaborane- κ^2^<i>P</i>,<i>P</i>'][7,8-bis(diphenylphosphino)-7,8-dicarba-<i>nido</i>- undecaborato-κ^2^<i>P</i>,<i>P</i>']gold(I)‒dichloromethane‒ water (2/1/1)
• Formula: C52.5 H62 Au B19 Cl O0.5 P4
• Calculated formula: C52.5 H61 Au B19 Cl O0.5 P4
• Title of publication: [1,2-Bis(diphenylphosphino)-1,2-dicarba-<i>closo</i>-dodecaborane-κ^2^<i>P</i>,<i>P</i>'][7,8-bis(diphenylphosphino)-7,8-dicarba-<i>nido</i>-undecaborato-κ^2^<i>P</i>,<i>P</i>']gold(I)‒dichloromethane‒water (2/1/1)
• Authors of publication: Ioppolo, Joseph A.; Clegg, Jack K.; Rendina, Louis M.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2009
• Journal volume: 65
• Journal issue: 5
• Pages of publication: m603 - m604
• a: 13.2043 ± 0.0006 Å
• b: 20.1424 ± 0.0009 Å
• c: 23.5721 ± 0.0011 Å
• α: 102.131 ± 0.003°
• β: 90.849 ± 0.003°
• γ: 105.839 ± 0.002°
• Cell volume: 5879.3 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0763
• Residual factor for significantly intense reflections: 0.0441
• Weighted residual factors for significantly intense reflections: 0.0865
• Weighted residual factors for all reflections included in the refinement: 0.0935
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes