Information card for entry 2222009

Structure parameters

• Chemical name: Bis[1,3(η^3^)-allyl][μ-2(η^4^)-1,3-bis(diphenylphosphino)-2,4- diphenylcyclobuta-1,3-diene-κ^2^<i>P</i>:<i>P</i>']dichlorido- 1κ<i>Cl</i>,3κ<i>Cl</i>-[2(η^5^)-isopropylcyclopentadienyl]-2- cobalt(I)-1,3-dipalladium(II) dichloromethane solvate
• Formula: C55 H53 Cl4 Co P2 Pd2
• Calculated formula: C55 H53 Cl4 Co P2 Pd2
• Title of publication: Bis[1,3(η^3^)-allyl][μ-2(η^4^)-1,3-bis(diphenylphosphino)-2,4-diphenylcyclobuta-1,3-diene-1:3κ^2^<i>P</i>:<i>P</i>']dichlorido-1κ<i>Cl</i>,3κ<i>Cl</i>-[2(η^5^)-isopropylcyclopentadienyl]-2-cobalt(I)-1,3-dipalladium(II) dichloromethane solvate
• Authors of publication: Chang, Chin-Pei; Hong, Fung-E
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2009
• Journal volume: 65
• Journal issue: 6
• Pages of publication: m669
• a: 10.889 ± 0.004 Å
• b: 12.499 ± 0.004 Å
• c: 21.746 ± 0.008 Å
• α: 94.617 ± 0.007°
• β: 102.136 ± 0.007°
• γ: 115.166 ± 0.007°
• Cell volume: 2570.1 ± 1.6 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0872
• Residual factor for significantly intense reflections: 0.047
• Weighted residual factors for significantly intense reflections: 0.1076
• Weighted residual factors for all reflections included in the refinement: 0.1264
• Goodness-of-fit parameter for all reflections included in the refinement: 0.982
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes