Information card for entry 2222309

Structure parameters

• Chemical name: [μ-(4<i>S</i>,5<i>S</i>,15<i>S</i>,16<i>S</i>)-10,21-Di-<i>tert</i>-butyl- 4,5,15,16-tetraphenyl-3,6,14,17-tetraazatricyclo[17.3.1.1^8,12^]tetracosa- 1(23),8,10,12(24),19,21-hexaene-23,24-diolato- κ^8^<i>N</i>^3^,<i>N</i>^6^,<i>O</i>^23^,<i>O</i>^24^: <i>N</i>^14^<i>N</i>^17^,<i>O</i>^23^,<i>O</i>^24^]bis[(acetato- κ<i>O</i>)zinc(II)] ethanol disolvate
• Formula: C44 H60 N4 O8 Zn2
• Calculated formula: C44 H60 N4 O8 Zn2
• Title of publication: [μ-(4<i>S</i>,5<i>S</i>,15<i>S</i>,16<i>S</i>)-10,21-Di-<i>tert</i>-butyl-4,5,15,16-tetraphenyl-3,6,14,17-tetraazatricyclo[17.3.1.1^8,12^]tetracosa-1(23),8,10,12(24),19,21-hexaene-23,24-diolato-κ^8^<i>N</i>^3^,<i>N</i>^6^,<i>O</i>^23^,<i>O</i>^24^:<i>N</i>^14^<i>N</i>^17^,<i>O</i>^23^,<i>O</i>^24^]bis[(acetato-κ<i>O</i>)zinc(II)] ethanol disolvate
• Authors of publication: Fan, Li-Jing; Ma, Jian-Fang; Liu, Jie
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2009
• Journal volume: 65
• Journal issue: 7
• Pages of publication: m777 - m778
• a: 9.0566 ± 0.0003 Å
• b: 10.841 ± 0.0005 Å
• c: 14.2828 ± 0.0005 Å
• α: 71.246 ± 0.004°
• β: 86.514 ± 0.003°
• γ: 78.362 ± 0.003°
• Cell volume: 1300.56 ± 0.09 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1143
• Residual factor for significantly intense reflections: 0.0771
• Weighted residual factors for significantly intense reflections: 0.2332
• Weighted residual factors for all reflections included in the refinement: 0.253
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes