Information card for entry 2223478

Structure parameters

• Chemical name: 2,4,6,8-Tetrakis(2-methoxyphenyl)-3,7-diazabicyclo[3.3.1]nonan-9-one diethyl ether hemisolvate
• Formula: C74 H82 N4 O11
• Calculated formula: C74 H82 N4 O11
• Title of publication: 2,4,6,8-Tetrakis(2-methoxyphenyl)-3,7-diazabicyclo[3.3.1]nonan-9-one diethyl ether hemisolvate
• Authors of publication: Fun, Hoong-Kun; Yeap, Chin Sing; Rajesh, K.; Sarveswari, S.; Vijayakumar, V.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2009
• Journal volume: 65
• Journal issue: 10
• Pages of publication: o2486 - o2487
• a: 13.5607 ± 0.0002 Å
• b: 13.764 ± 0.0002 Å
• c: 20.3227 ± 0.0003 Å
• α: 90°
• β: 123.143 ± 0.001°
• γ: 90°
• Cell volume: 3176.1 ± 0.09 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0733
• Residual factor for significantly intense reflections: 0.0536
• Weighted residual factors for significantly intense reflections: 0.1314
• Weighted residual factors for all reflections included in the refinement: 0.1438
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes