Information card for entry 2224309

Structure parameters

• Chemical name: Bis[<i>N</i>,<i>N</i>'-bis(2,6-diisopropylphenyl)ethane-1,2-diimine]- 1κ^2^<i>N</i>,<i>N</i>';2κ^2^<i>N</i>,<i>N</i>'-tri-μ-trichlorido- 1:2κ^6^<i>Cl</i>:<i>Cl</i>- chlorido-1κ<i>Cl</i>-tetrahydrofuran-2κ<i>O</i>-dichromium(II) dichloromethane 4.5-solvate
• Formula: C98.5 H89 Cr2 N4 O
• Calculated formula: C60.5 H89 Cl13 Cr2 N4 O
• Title of publication: Bis[<i>N</i>,<i>N</i>'-bis(2,6-diisopropylphenyl)ethane-1,2-diimine]-1κ^2^<i>N</i>,<i>N</i>';2κ^2^<i>N</i>,<i>N</i>'-tri-μ-trichlorido-1:2κ^6^<i>Cl</i>:<i>Cl</i>-chlorido-1κ<i>Cl</i>-tetrahydrofuran-2κ<i>O</i>-dichromium(II) dichloromethane 4.5-solvate
• Authors of publication: Peitz, Stephan; Peulecke, Normen; Müller, Bernd H.; Spannenberg, Anke; Rosenthal, Uwe
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2009
• Journal volume: 65
• Journal issue: 12
• Pages of publication: m1574
• a: 18.2545 ± 0.0006 Å
• b: 15.4111 ± 0.0004 Å
• c: 27.3121 ± 0.0007 Å
• α: 90°
• β: 105.16 ± 0.002°
• γ: 90°
• Cell volume: 7416.1 ± 0.4 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0677
• Residual factor for significantly intense reflections: 0.0443
• Weighted residual factors for significantly intense reflections: 0.1164
• Weighted residual factors for all reflections included in the refinement: 0.1225
• Goodness-of-fit parameter for all reflections included in the refinement: 0.929
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes