Information card for entry 2224673

Structure parameters

• Chemical name: Bis[μ-2-(2,4-difluorophenyl)-1,3-bis(1,2,4-triazol-1-yl)propan-2-olato- κ^4^<i>N</i>^2^,<i>O</i>:<i>O</i>,<i>N</i>^2'^]bis[(acetato- κ^2^<i>O</i>,<i>O</i>')nickel(II)] methanol hemisolvate
• Formula: C30.5 H30 F4 N12 Ni2 O6.5
• Calculated formula: C30.5 H30 F4 N12 Ni2 O6.5
• Title of publication: Bis[μ-2-(2,4-difluorophenyl)-1,3-bis(1,2,4-triazol-1-yl)propan-2-olato-κ^4^<i>N</i>^2^,<i>O</i>:<i>O</i>,<i>N</i>^2'^]bis[(acetato-κ^2^<i>O</i>,<i>O</i>')nickel(II)] methanol hemisolvate
• Authors of publication: Zhang, Feng; Hu, Fei-Long; Huang, Zhong-Jing; Zhuang, Ji-Chang; Zhuang, Yue
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2010
• Journal volume: 66
• Journal issue: 1
• Pages of publication: m75 - m76
• a: 11.3898 ± 0.0012 Å
• b: 12.4447 ± 0.0014 Å
• c: 14.0012 ± 0.0016 Å
• α: 65.211 ± 0.001°
• β: 86.815 ± 0.002°
• γ: 88.1 ± 0.002°
• Cell volume: 1798.8 ± 0.3 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.066
• Residual factor for significantly intense reflections: 0.0427
• Weighted residual factors for significantly intense reflections: 0.1071
• Weighted residual factors for all reflections included in the refinement: 0.1272
• Goodness-of-fit parameter for all reflections included in the refinement: 0.966
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes