Information card for entry 2224686

Structure parameters

• Chemical name: 6-(1-Methylethyl)-12-phenyl-5,6,7,12- tetrahydrodibenz[<i>c</i>,<i>f</i>][1,5]azasilocine
• Formula: C23 H25 N Si
• Calculated formula: C23 H25 N Si
• SMILES: [SiH]1(c2c(cccc2)CN(Cc2c1cccc2)C(C)C)c1ccccc1
• Title of publication: 6-(1-Methylethyl)-12-phenyl-5,6,7,12-tetrahydrodibenz[<i>c</i>,<i>f</i>][1,5]azasilocine
• Authors of publication: Goto, Kei; Fukushima, Akihiro; Kawashima, Takayuki
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2010
• Journal volume: 66
• Journal issue: 1
• Pages of publication: o20
• a: 9.756 ± 0.007 Å
• b: 10.269 ± 0.007 Å
• c: 18.912 ± 0.012 Å
• α: 90°
• β: 92.745 ± 0.003°
• γ: 90°
• Cell volume: 1893 ± 2 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0502
• Residual factor for significantly intense reflections: 0.0411
• Weighted residual factors for significantly intense reflections: 0.0941
• Weighted residual factors for all reflections included in the refinement: 0.1002
• Goodness-of-fit parameter for all reflections included in the refinement: 1.083
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes