Information card for entry 2225541

Structure parameters

• Chemical name: Di-μ-chlorido-bis{[μ-1,8-bis(diisopropylphosphanyl)-9,10-dihydro- 9,10-ethanoanthracene-κ^2^<i>P</i>:<i>P</i>']-μ-chlorido-μ-methylidene- dipalladium(II)} tetrahydrofuran pentasolvate
• Formula: C78 H124 Cl4 O5 P4 Pd4
• Calculated formula: C78 H124 Cl4 O5 P4 Pd4
• Title of publication: Di-μ-chlorido-bis{[μ-1,8-bis(diisopropylphosphanyl)-9,10-dihydro-9,10-ethanoanthracene-κ^2^<i>P</i>:<i>P</i>']-μ-chlorido-μ-methylidene-dipalladium(II)} tetrahydrofuran pentasolvate
• Authors of publication: Schnetz, Thomas; Rominger, Frank; Hofmann, Peter
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2010
• Journal volume: 66
• Journal issue: 4
• Pages of publication: m453 - m454
• a: 12.5799 ± 0.0001 Å
• b: 17.283 ± 0.0003 Å
• c: 19.7558 ± 0.0002 Å
• α: 79.877 ± 0.001°
• β: 74.703 ± 0.001°
• γ: 80.717 ± 0.001°
• Cell volume: 4048.61 ± 0.09 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0999
• Residual factor for significantly intense reflections: 0.0466
• Weighted residual factors for significantly intense reflections: 0.0879
• Weighted residual factors for all reflections included in the refinement: 0.1055
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes