Information card for entry 2226125

Structure parameters

• Common name: 2-Chloro-2-methyl-1,1-diphenyl-3-[2-(2-thienyl)ethyl]-1<i>H</i>- 1λ^4^-aza-3-phospha-2-palladanaphthalene dichloromethane hemisolvate
• Chemical name: Chlorido{<i>N</i>-[2-(diphenylphosphanyl)benzylidene]-2-(2-thienyl)ethanamine- κ^2^<i>N</i>,<i>P</i>}methylpalladium(II) dichloromethane hemisolvate
• Formula: C26.5 H26 Cl2 N P Pd S
• Calculated formula: C26.5 H26 Cl2 N P Pd S
• Title of publication: Chlorido{<i>N</i>-[2-(diphenylphosphanyl)benzylidene]-2-(2-thienyl)ethanamine-κ^2^<i>N</i>,<i>P</i>}methylpalladium(II) dichloromethane hemisolvate
• Authors of publication: Onani, Martin O.; Motswainyana, William M.; Iwuoha, Emmanuel I.; Darkwa, James; Lalancette, Roger A.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2010
• Journal volume: 66
• Journal issue: 6
• Pages of publication: m688
• a: 9.996 ± 0.0006 Å
• b: 18.6584 ± 0.0011 Å
• c: 13.8167 ± 0.0008 Å
• α: 90°
• β: 94.517 ± 0.001°
• γ: 90°
• Cell volume: 2568.9 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0351
• Residual factor for significantly intense reflections: 0.029
• Weighted residual factors for significantly intense reflections: 0.0703
• Weighted residual factors for all reflections included in the refinement: 0.0739
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes