Information card for entry 2226992

Structure parameters

• Chemical name: Bis[2,6-bis(1<i>H</i>-benzimidazol-2-yl)pyridine]nickel(II) dipicrate dimethylformamide disolvate
• Formula: C56 H44 N18 Ni O16
• Calculated formula: C56 H44 N18 Ni O16
• Title of publication: Bis[2,6-bis(1<i>H</i>-benzimidazol-2-yl)pyridine]nickel(II) dipicrate dimethylformamide disolvate
• Authors of publication: Huang, Xingcai; Kou, Fan; Qi, Baoliang; Meng, Xuan; Wu, Huilu
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2010
• Journal volume: 66
• Journal issue: 8
• Pages of publication: m967
• a: 14.2087 ± 0.0003 Å
• b: 26.5215 ± 0.0005 Å
• c: 14.6989 ± 0.0003 Å
• α: 90°
• β: 93.775 ± 0.001°
• γ: 90°
• Cell volume: 5527.06 ± 0.19 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0605
• Residual factor for significantly intense reflections: 0.0399
• Weighted residual factors for significantly intense reflections: 0.092
• Weighted residual factors for all reflections included in the refinement: 0.1062
• Goodness-of-fit parameter for all reflections included in the refinement: 1.108
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes