Information card for entry 2227313

Structure parameters

• Chemical name: Di-μ-azido-κ^4^<i>N</i>^1^:<i>N</i>^1^-bis[(1,10-phenanthroline- κ^2^<i>N</i>,<i>N</i>')(thiocyanato-κ<i>N</i>)lead(II)]
• Formula: C50 H32 N16 Pb2 S2
• Calculated formula: C50 H32 N16 Pb2 S2
• SMILES: [N]1(=N#N)[Pb]23(N=C=S)([n]4c5c(ccc4)ccc4ccc[n]2c45)([n]2c4c(ccc2)ccc2ccc[n]3c24)[N](=N#N)[Pb]123(N=C=S)([n]1c4c(ccc1)ccc1ccc[n]2c14)[n]1c2c(ccc1)ccc1ccc[n]3c12
• Title of publication: Di-μ-azido-κ^4^<i>N</i>^1^:<i>N</i>^1^-bis[(1,10-phenanthroline-κ^2^<i>N</i>,<i>N</i>')(thiocyanato-κ<i>N</i>)lead(II)]
• Authors of publication: Mohammadnezhad, Gholamhossein; Ghanbarpour, Ali Reza; Amini, Mostafa M.; Ng, Seik Weng
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2010
• Journal volume: 66
• Journal issue: 9
• Pages of publication: m1120
• a: 10.3412 ± 0.0006 Å
• b: 10.8327 ± 0.0006 Å
• c: 11.4178 ± 0.0006 Å
• α: 89.923 ± 0.001°
• β: 72.08 ± 0.001°
• γ: 65.273 ± 0.001°
• Cell volume: 1093.35 ± 0.11 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0214
• Residual factor for significantly intense reflections: 0.0198
• Weighted residual factors for significantly intense reflections: 0.0606
• Weighted residual factors for all reflections included in the refinement: 0.0612
• Goodness-of-fit parameter for all reflections included in the refinement: 1.088
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes