Information card for entry 2227673

Structure parameters

• Chemical name: <i>catena</i>-Poly[[(tetrahydrofuran-κ<i>O</i>)lithium(I)]- bis(μ-trimethylsilanolato-κ^2^<i>O</i>:<i>O</i>)-gallium(III)- bis(μ-trimethylsilanolato-κ^2^<i>O</i>:<i>O</i>)- [(tetrahydrofuran-κ<i>O</i>)lithium(I)]-μ-bromido]
• Formula: C20 H52 Br Ga Li2 O6 Si4
• Calculated formula: C20 H52 Br Ga Li2 O6 Si4
• Title of publication: <i>catena</i>-Poly[[(tetrahydrofuran-κ<i>O</i>)lithium(I)]-bis(μ-trimethylsilanolato-κ^2^<i>O</i>:<i>O</i>)-gallium(III)-bis(μ-trimethylsilanolato-κ^2^<i>O</i>:<i>O</i>)-[(tetrahydrofuran-κ<i>O</i>)lithium(I)]-μ-bromido]
• Authors of publication: Grubba, Rafał; Baranowska, Katarzyna; Pikies, Jerzy
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2010
• Journal volume: 66
• Journal issue: 10
• Pages of publication: m1242
• a: 25.802 ± 0.008 Å
• b: 9.761 ± 0.002 Å
• c: 18.689 ± 0.006 Å
• α: 90°
• β: 130.81 ± 0.02°
• γ: 90°
• Cell volume: 3563 ± 2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0325
• Residual factor for significantly intense reflections: 0.0308
• Weighted residual factors for significantly intense reflections: 0.0828
• Weighted residual factors for all reflections included in the refinement: 0.0841
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes