Information card for entry 2228635

Structure parameters

• Chemical name: [<i>N</i>,<i>N</i>'-Bis(2,6-diisopropylphenyl)methanimidamidato][η^8^- 1,4-bis(trimethylsilyl)cyclooctatetraenyl](tetrahydrofuran)samarium(III) toluene monosolvate
• Formula: C50 H75 N2 O Si2 Sm
• Calculated formula: C50 H74.4 N2 O Si2 Sm
• Title of publication: [<i>N</i>,<i>N</i>'-Bis(2,6-diisopropylphenyl)methanimidamidato][η^8^-1,4-bis(trimethylsilyl)cyclooctatetraenyl](tetrahydrofuran)samarium(III) toluene monosolvate
• Authors of publication: Edelmann, Anja; Hrib, Cristian G.; Hilfert, Liane; Blaurock, Steffen; Edelmann, Frank T.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2010
• Journal volume: 66
• Journal issue: 12
• Pages of publication: m1675 - m1676
• a: 18.49 ± 0.004 Å
• b: 11.166 ± 0.002 Å
• c: 24.865 ± 0.005 Å
• α: 90°
• β: 107.8 ± 0.03°
• γ: 90°
• Cell volume: 4887.9 ± 1.9 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0336
• Residual factor for significantly intense reflections: 0.0243
• Weighted residual factors for significantly intense reflections: 0.0549
• Weighted residual factors for all reflections included in the refinement: 0.0562
• Goodness-of-fit parameter for all reflections included in the refinement: 0.895
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes