Information card for entry 2228832

Structure parameters

• Chemical name: Bis(tri-2-pyridylamine)nickel(II) bis(perchlorate)
• Formula: C30 H24 Cl2 N8 Ni O8
• Calculated formula: C30 H24 Cl2 N8 Ni O8
• Title of publication: Bis(tri-2-pyridylamine)nickel(II) bis(perchlorate)
• Authors of publication: Wang, Shi; He, Wenrui; Huang, Wei
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2011
• Journal volume: 67
• Journal issue: 1
• Pages of publication: m78
• a: 8.36 ± 0.004 Å
• b: 17.57 ± 0.008 Å
• c: 11.165 ± 0.005 Å
• α: 90°
• β: 99.542 ± 0.005°
• γ: 90°
• Cell volume: 1617.3 ± 1.3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0704
• Residual factor for significantly intense reflections: 0.0394
• Weighted residual factors for significantly intense reflections: 0.0864
• Weighted residual factors for all reflections included in the refinement: 0.0964
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes