Information card for entry 2229343

Structure parameters

• Chemical name: Acetonitrile[2-(1-{bis[2,4,6-tris(trifluoromethyl)phenyl]phosphanyloxy}- 1-methylethyl)pyridine]methylpalladium(II) hexafluoridoantimonate dichloromethane hemisolvate
• Formula: C29.5 H21 Cl F24 N2 O P Pd Sb
• Calculated formula: C29.5 H21 Cl F24 N2 O P Pd Sb
• Title of publication: Acetonitrile[2-(1-{bis[2,4,6-tris(trifluoromethyl)phenyl]phosphanyloxy}-1-methylethyl)pyridine]methylpalladium(II) hexafluoridoantimonate dichloromethane hemisolvate
• Authors of publication: Li, Liuzhong; White, Peter S.; Hao, Aiyou
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2011
• Journal volume: 67
• Journal issue: 3
• Pages of publication: m365
• a: 8.8635 ± 0.0008 Å
• b: 12.1336 ± 0.0012 Å
• c: 19.107 ± 0.002 Å
• α: 79.166 ± 0.008°
• β: 80.147 ± 0.008°
• γ: 78.266 ± 0.008°
• Cell volume: 1957.1 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0863
• Residual factor for significantly intense reflections: 0.0664
• Weighted residual factors for significantly intense reflections: 0.1758
• Weighted residual factors for all reflections included in the refinement: 0.1914
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes