Information card for entry 2230586

Structure parameters

• Chemical name: Bis[μ-<i>N</i>'-(2-oxidobenzylidene)thiophene-2- carbohydrazidato]bis[dimethanolnickel(II)]
• Formula: C28 H32 N4 Ni2 O8 S2
• Calculated formula: C28 H32 N4 Ni2 O8 S2
• Title of publication: Bis[μ-<i>N</i>'-(2-oxidobenzylidene)thiophene-2-carbohydrazidato]bis[dimethanolnickel(II)]
• Authors of publication: Ma, Jian-Hua; Wu, Wen-Shi; Zhang, Xiao-Qing; Tang, Sheng-Jiao; Lin, Xin-Yong
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2011
• Journal volume: 67
• Journal issue: 7
• Pages of publication: m910
• a: 13.7958 ± 0.0014 Å
• b: 7.888 ± 0.0008 Å
• c: 14.4219 ± 0.0016 Å
• α: 90°
• β: 104.672 ± 0.001°
• γ: 90°
• Cell volume: 1518.2 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0431
• Residual factor for significantly intense reflections: 0.037
• Weighted residual factors for significantly intense reflections: 0.0857
• Weighted residual factors for all reflections included in the refinement: 0.0888
• Goodness-of-fit parameter for all reflections included in the refinement: 1.112
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes