Information card for entry 2230903

Structure parameters

• Chemical name: μ-oxido-bis[bis(<i>N</i>,<i>N</i>-diethylhydroxylaminato)oxidovanadium(V)]
• Formula: C16 H40 N4 O7 V2
• Calculated formula: C16 H40 N4 O7 V2
• SMILES: C(C)[N]1(CC)O[V]21([N](CC)(CC)O2)(O[V]12([N](CC)(CC)O1)([N](CC)(CC)O2)=O)=O
• Title of publication: Redetermination of μ-oxido-bis[bis(<i>N</i>,<i>N</i>-diethylhydroxylaminato)oxidovanadium(V)]
• Authors of publication: Zhang, Heng-Qiang; Jin, Zhong-Min; Fan, Xin; Zhang, Qi-Ying
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2011
• Journal volume: 67
• Journal issue: 7
• Pages of publication: m860 - m861
• a: 14.6106 ± 0.0003 Å
• b: 10.2624 ± 0.0002 Å
• c: 19.4547 ± 0.0003 Å
• α: 90°
• β: 120.744 ± 0.001°
• γ: 90°
• Cell volume: 2507.07 ± 0.08 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0376
• Residual factor for significantly intense reflections: 0.0302
• Weighted residual factors for significantly intense reflections: 0.0859
• Weighted residual factors for all reflections included in the refinement: 0.0896
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes