A monoclinic polymorph with <i>Z</i> = 4 of (<i>E</i>)-2,4-dihydroxyacetophenone 2,4-dinitrophenylhydrazone <i>N</i>,<i>N</i>-dimethylformamide monosolvate
Authors of publication
Han, Hongfei; Liu, Yaohua
Journal of publication
Acta Crystallographica Section E
Year of publication
2011
Journal volume
67
Journal issue
12
Pages of publication
o3434
a
6.7546 ± 0.0006 Å
b
20.9647 ± 0.0018 Å
c
13.3508 ± 0.0013 Å
α
90°
β
99.772 ± 0.001°
γ
90°
Cell volume
1863.2 ± 0.3 Å3
Cell temperature
298 ± 2 K
Ambient diffraction temperature
298 ± 2 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.1073
Residual factor for significantly intense reflections
0.0522
Weighted residual factors for significantly intense reflections
0.1188
Weighted residual factors for all reflections included in the refinement
0.1418
Goodness-of-fit parameter for all reflections included in the refinement