Information card for entry 2232678

Structure parameters

• Chemical name: Bis[tris(ethylenediamine-κ^2^<i>N</i>,<i>N</i>')cobalt(III)] octakis-μ-~3~-oxido-hexadeca-μ~2~-oxido-tetradecaoxido-μ~12~- tetraoxosilicato-octamolybdenum(VI)hexavanadium(IV,V) hexahydrate
• Formula: C12 H60 Co2 Mo8 N12 O48 Si V6
• Calculated formula: C12 H48 Co2 Mo8 N12 O48 Si V6
• Title of publication: Bis[tris(ethylenediamine-κ^2^<i>N</i>,<i>N</i>')cobalt(III)] octakis-μ-~3~-oxido-hexadeca-μ~2~-oxido-tetradecaoxido-μ~12~-tetraoxosilicato-octamolybdenum(VI)hexavanadium(IV,V) hexahydrate
• Authors of publication: Lu, Yu-Kun; Tian, Ming-Ming; Xu, Shu-Gang; Lü, Ren-Qing; Liu, Yun-Qi
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2011
• Journal volume: 67
• Journal issue: 12
• Pages of publication: m1776 - m1777
• a: 20.744 ± 0.004 Å
• b: 21.498 ± 0.004 Å
• c: 13.623 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6075 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0794
• Residual factor for significantly intense reflections: 0.0537
• Weighted residual factors for significantly intense reflections: 0.1208
• Weighted residual factors for all reflections included in the refinement: 0.1333
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes